GCMS surrogate recovery results, sample AE07114, April 16, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\MSDCHEM\l\DATA\041002\7114.D Vial:. 21 Acq On : 11 Apr 2002 6:26 am Operator: Bohllc Sample : SAMPLE 7114 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 1 Cyclopentasiioxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.92 4.38 ug/L 523591 Naphthalene-d8 12.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiioxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Cyclopentasiioxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 40 4 M-HYDROXYPHENETHANOL 2TMS 282 C14H26O2Si2 000000-00-0 40 Abundance Scan 1505 (11.922 min): 7114.D (-) rm/z 73710 100.00% 73

5000 267 355 11.60 11.80 12.00 12.20 323 t 0 ^44 125 IM 191 223 m/z 267.00 25.19% •n/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiioxane, decamethyl-’ 7(3

5000 267 11.60 11.80 12.00 12.20 355 m/z 355.00 14.78% 45 28 ,1. I 96 133 165 ,223 247 293 323 i 0 ' ' ’n—’■ ' T' •n/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiioxane, decamettiyl- 713

355 11.60 11.80 12.00 12.20 267 m/z 74.10 8.93% 5000

45 207 323 oi I I ' m/z-> 50 100 150 200 250 300 350 Abundance #362614: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 7(3 T 11.60 11.80 12.00 12.20 m/z 268.00 5.80%

5000 267 44

0 1 , 1I". ,104 131151 179 ^09 237 I ' ■' i ' I I ' ■n/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

'114.D 5080402BB.M Mon Apr 15 18:08:22 2002 Page 3

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