GCMS analysis report, sample AE07172, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7172.D Vial: 25 Acq On : 11 Apr 2002 9:43 am Operator: Bohlk Sample : SAMPLE 7172 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiioxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.92 2.80 ug/L 372961 Naphthalene-d8 12.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiioxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiioxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 38 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 38 /Abundance Scan 1505 (11.922 min): 7172.D (-) m/z 73.10 100.00% 73

5000

267 ............................................ 355 11.60 11:80 12.00 12.20 108 154 193 223 323 [ m/z 267.00 25.13% 0^ ■ t'' ' ' I ' m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiioxane, decamethyl- 73

. 355 267 5000 11.60 11.80 12.00 12.20 m/z 355.10 16.23% 45 207 ■ 323 [ ......................... 0^ •n/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiioxane, decamethyl- 73

T 11.60 11.80 12.00 12.20 5000 m/z 74.10 8.76% 267 355 45 103 1331165, ^^,223 293 323 0^ '' ’ ' i ' ■n/z-> 50 100 150 200 250 300 350 400 450 Abundance #361636: 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 7i3 11.60 11.80 12.00 12.20 m/z 356.00 6.45%

355 5000

45 0 I, 147 I 193 267 295 429 457 ' I ' ' ' ' I ' ' ' ' I ' ■n/z-> 50 100 150 200 250 300 350 400 450 11.60 11.80 12.00 12.20

7172.D 5080402BB.M Mon Apr 15 18:35:49 2002 Page 3

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