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GCMS analysis results for sample AE06635, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.

NYC-WTC_000060478–000060494

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000060489
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR1602\6635.D Vial: 8 Acq On 16 Apr 2002 8:03 pm Operator: Sample gc/ms scan 3/22. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 37.32 3.62 ug/1 439537 Perylene-dl2 37.88 Hit# of 5 Tenl/ative ID MW MolForm • CAS# Qual _ _ /__________ 1 l,l,l,5,7,7,yHeptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 28 2 1,2-Benzene^icarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 14 3 Benzoic aci^, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 10 4 Trisiloxang, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 10 Abundance Scan 3515 (37.316 min); 6635. D (-) 73.00 100.00%! 7)3

147 5000 221 355 281 429 37.00 37.20 37.40 37.60 44 'p'"I 96 117 I'" ' 1' I'''' I' L m/z 147.0062.07% ttZz~> 40 60 80 100120140160180200 220240260280300320340360380400 420 Abundance #56714; 1,1,1,5.7,7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73

147 5000 267 355 37.00 37.20 37.40 37.60 429 45 207 m/z 221.05 46760% J L .. I I'" ' p ''' I I" " I ‘‘ I I " " I" " I P ■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 1 17 ' ‘ 1 ' ' ' ' I. ' 73 37.00 37.20 37.40 37.60 5000 m/z 355.05 29.14% 45 295

■n/z-> 1 Ir -ph-1

40 60 80 100120140160180200220240260280300320340360380400420 I " '' I'' ‘' I p

Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls —I I 11 I I 11 73 37.00 37.20 37.40 37.60 355 m/z 281.00 23.95% 5000

45

I.. I .... ,.f 1,79.. ,... , 297....... mfe-> 40 60 80 100120140160180200220240260280 300320340360 380 400 420 37 00 37 20 37.40 37.60

6635.D GCMS0412.M Wed Apr 17 12:03:08 2002 Page 5

NYC-WTC_000060489

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NYC-WTC_000060489Source: NYC Law Department, mirrored locally

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