NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\APR1602\6635.D Vial: 8
Acq On 16 Apr 2002 8:03 pm Operator:
Sample gc/ms scan 3/22. Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
37.32 3.62 ug/1 439537 Perylene-dl2 37.88
Hit# of 5 Tenl/ative ID MW MolForm • CAS# Qual
_ _ /__________
1 l,l,l,5,7,7,yHeptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 28
2 1,2-Benzene^icarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 14
3 Benzoic aci^, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 10
4 Trisiloxang, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 10
Abundance Scan 3515 (37.316 min); 6635. D (-) 73.00 100.00%!
7)3
147
5000 221
355
281
429 37.00 37.20 37.40 37.60
44
'p'"I
96 117
I'" ' 1' I'''' I'
L m/z 147.0062.07%
ttZz~> 40 60 80 100120140160180200 220240260280300320340360380400 420
Abundance #56714; 1,1,1,5.7,7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t
73
147
5000 267
355 37.00 37.20 37.40 37.60
429
45 207 m/z 221.05 46760%
J
L
.. I
I'" ' p ''' I I" " I ‘‘ I I " " I" " I P
■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e
1 17
' ‘ 1 ' ' ' ' I. '
73 37.00 37.20 37.40 37.60
5000 m/z 355.05 29.14%
45 295
■n/z->
1 Ir
-ph-1
40 60 80 100120140160180200220240260280300320340360380400420
I " '' I'' ‘' I p
Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls —I I 11 I I 11
73 37.00 37.20 37.40 37.60
355 m/z 281.00 23.95%
5000
45
I.. I .... ,.f 1,79.. ,... , 297.......
mfe-> 40 60 80 100120140160180200220240260280 300320340360 380 400 420 37 00 37 20 37.40 37.60
6635.D GCMS0412.M Wed Apr 17 12:03:08 2002 Page 5
NYC-WTC_000060489
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