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GCMS reference analysis results for sample AE06090, April 2002

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Laboratory report documenting reference standard analysis for organic compounds in sample AE06090 conducted on April 18, 2002.

NYC-WTC_000059998–000060006

Folder label: “GCMS X 3/15/02 A 4/5/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6090.D Vial: 13 Acq On 5 Apr 2002 5:18 am Operator: Bohlk Sample SAMPLE 6090 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyciopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 1.25 ug/L 671925 Naphthalene-d8 12.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyciopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Cyciopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 4 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 40 <Kbundance Scan 1514(11.975 min): 6090.D (-) m/z 73.10 100.00% 73

Tom 267 355 11.60 11.80 12.00 12.20 108 1^ 193223 . 323 m/z 267.00 28.79% m/z-> OU 4^ 50 '' I' ' ■'' r'' ’ i"' ' f' 100 150 200 250 300 350 400 450 500 550 /Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 T" 11.60 11.80 12.00 12.20 m/z 355.00 17.45%

I , .207 4 323^ 0( m/z-> 50 100 150 200 250 300 350 400 450 500 550 ^Abundance #313065: Cyciopentasiloxane, decamelhyl- 7i3 /

11.60 11.80 12.00 12.20 5000 m/z 74.10 8.02% 267 355

103133163,^?3223 j 323 0 -ri-rt-r I ' ' ' H m/z-> 50 100 150 200 250 300 350 400 450 500 550 /Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methyien...

355 11.60 11.80 12.00 12.20 m/z 356.10 6.87%'

5000

117.147177207 251281 oL-4^ l-ii r, '1 r. I I* IA (. . (. I f. I 386 458 548 ■T T ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 Iteoiljo 12.00 12.20

5090.D 5080402.M Fri Apr 05 06:45:48 2002 Page 3

NYC-WTC_000060005

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NYC-WTC_000060005Source: NYC Law Department, mirrored locally

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