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GCMS reference data for sample AE05847, April 16 2002

Machine-extracted title · confidence 90%

Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.

NYC-WTC_000059608–000059618

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0402\5847.D Vial: 21 Acq On 4 Apr 2002 5:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0468.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF ■Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.761 295 296 298 rBV 51672 29289 1.09% 0.236% 2 8.128 331 336 347 rBV 139336 369520 13.72% 2.983% 3 8.275 349 352 360 rVB 17133 45963 1.71% 0.371% 4 12.250 779 785 804 rBV 725767 1845905 68.54% 14.902% 5 15.885 1175 1181 1199 rBV 1096364 2350923 87.29% 18.978%

6 21.182 1752 1758 1772 rBV 1283270 2693357 100.00% 21.743% 7 25.625 2236 2242 2254 rBV2 1138372 2440725 90.62% 19.703% 8 27.599 2452 2457 2462 rBV 60129 108687 4.04% 0.877% 9 30.702 2790 2795 2802 rBV 175561 347691 12.91% 2.807% 10 33.686 3114 3120 3135 rBV2 592677 1322917 49.12% 10.680%

11 37.927 3574 3582 3596 rBV2 273498 832327 30.90% 6.719%

Sum of corrected areas: 12387304

5847.D GCMS0408.M Tue Apr 16 08:17:06 2002

NYC-WTC_000059613

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NYC-WTC_000059613Source: NYC Law Department, mirrored locally

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