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GCMS analysis results for sample AE05851, April 17 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE05851 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059650–000059659

Folder label: “GCMS X 3/12/02 A 4/4/02

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Scanned page image, NYC-WTC_000059655
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0402\5851.D Vial: 25 Acq On 4 Apr 2002 9:45 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 . Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.127 331 336 349 rBV 121738 347868 12.35% 2.704% 2 8.274 349 352 362 rVB 15849 46179 1.64% 0.359% 3 12.240 779 784 802 rVB 734981 1935134 68.72% 15.041% 4 15.885 1175 1181 1198 rBV 1155193 2465890 87.57% 19.166% 5 21.182 1752 1758 1779 rBV 1316202 2815954 100.00% 21.887%

6 25.625 2236 2242 2253 rBV2 1175495 2559310 90.89% 19.892% 7 27.599 2452 2457 2464 rVB 36907 69445 2.47% 0.540% 8 30.702 2790 2795 2801 rBV 184699 361021 12.82% 2.806% 9 33.685 3113 3120 3135 rBV2 618399 1373771 48.79% 10.677% 10 37.927 3574 3582 3602 rBV 300440 891466 31.66% 6.929%

Sum of corrected areas: 12866038

5851.D GCMS0408.M Tue Apr 16 08:18:06 2002

NYC-WTC_000059655

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NYC-WTC_000059655Source: NYC Law Department, mirrored locally

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