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GCMS analysis results for sample AE05847, April 17 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05847 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059619–000059628

Folder label: “GCMS X 3/12/02 A 4/4/02

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Scanned page image, NYC-WTC_000059624
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0402\5848.D Vial: 22 Acq On 4 Apr 2002 6:47 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1% of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.119 331 335 349 rBV 117807 338609 13.12% 2.848% 2 8.275 349 3 52 361 rVB2 17697 49615 1.92% 0.417% 3 12.241 779 784 802 rVB 687436 1791773 69.44% 15.070% 4 15.886 1175 1181 1198 rBV 1047368 2279584 88.34% 19.173% 5 21.183 i752 1758 1768 rBV 1241101 2580443 100.00% 21.703% 6 25.626 2236 2242 2252 rBV2 1110251 2353167 91.19% 19.791% 7 27.600 2451 2457 2461 rBV 42360 80434 3.12% 0.676% 8 30.703 2790 2795 2802 rBV 175419 347718 13.48% 2.924% 9 33.686 3113 3120 3139 rBV 570170 1269366 49.19% 10.676% 10 37.928 3575 3582 3600 rBV 262644 799136 30.97% 6.721%

Sum of corrected areas; 11889845 5848.D GCMS0408.M Tue Apr 16 08:17:21 2002

NYC-WTC_000059624

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NYC-WTC_000059624Source: NYC Law Department, mirrored locally

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