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GCMS analysis results for sample AE05849, April 17 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05849 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059639–000059649

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR0 4 0 2\5 8 5 0.D Vial: 24 Acq On 4 Apr 2002 8:46 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.122 331 335 349 rBV 139580 382984 13.89% 3.014% 2 8.269 349 351 361 rVB 14327 42568 1.54% 0.335% 3 12.244 779 784 799 rBV 754521 1882609 68.27% 14.815% 4 15.879 1174 1180 1198 rBV 1164698 2426430 88.00% 19.094% 5 21.075 1741 1746 1752 rBV2 17987 32836 1.19% 0.258%

6 21.186 1752 1758 1774 rBV 1372793 2757417 100.00% 21.699% 7 25.629 2235 2242 2254 rBV2 1209973 2493095 90.41% 19.619% 8 27.593 2451 2456 2461 rBV 40542 78803 2.86% 0.620% 9 30.706 2790 2795 2800 rBV 194495 369402 13.40% 2.907% 10 33.689 3113 3120 3132 rBV 588631 1370272 49.69% 10.783%

11 37.931 3574 3582 3597 rBV 288609 871255 31.60% 6.856%

Sum of corrected areas: 12707671

5850.D GCMS0408.M Tue Apr 16 08:17:51 2002

NYC-WTC_000059644

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NYC-WTC_000059644Source: NYC Law Department, mirrored locally

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