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GCMS analysis results for sample AE05846, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE05846 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048717–000048736

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\APR0402\5846A.D Vial: 20 Acq On 4 Apr 2002 4:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.127 332 336 350 rBV 114082 318708 12.32% 2.717% 2 8.274 350 352 363 rVB 11559 31207 1.21% 0.266% 3 12.249 779 785 799 rBV 666828 1743892 67.43% 14.868% 4 15.884 1175 1181 1196 rBV 1051651 2255562 87.21% 19.230% 5 21.181 1752 1758 1770 rBV 1219725 2586247 100.00% 22.050% 6 25.625 2236 2242 2255 rBV2 1076820 2329974 90.09% 19.865% 7 27.598 2452 2457 2462 rBV 69465 129737 5.02% 1.106% 8 30.701 2790 2795 2802 rVB 153549 304082 11.76% 2.593% 9 33.685 3114 3120 3133 rBV2 547773 1234101 47.72% 10.522% 10 37.926 3575 3582 3598 rBV2 255688 767082 29.66% 6.540% 11 43.444 4181 4183 4185 rBV 48466 28517 1.10% 0.243%

Sum of corrected areas: 11729109 5846A.D GCMS0408.M Tue Apr 16 08:16:48 2002

NYC-WTC_000048731

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NYC-WTC_000048731Source: NYC Law Department, mirrored locally

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