GCMS calibration scan data, Sample 5844, April 4 2002

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LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APRO 3022\5750.D Vial: 17 Acq On 4 Apr 2002 11:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.124 330 335 343 rBV 131714 344241 13.65% 2.595% 2 8.225 343 346 364 rVB2 34121 132081 5.24% 0.996% 3 12.246 778 784 800 rBV 649969 1722532 68.31% 12.987% 4 15.882 1174 1180 1198 rBV 1049114 2214096 87.81% 16.694% 5 21.078 1740 1746 1751 rBV 17715 33805 1.34% 0.255%

6 21.188 1751 1758 1776 rBV 1236636 2521553 100.00% 19.012% 7 25.631 2235 2242 2253 rBV2 1059667 2305296 91.42% 17.381% 8 27.596 2451 2456 2470 rBV 843693 1564677 62.05% 11.797% 9 30.708 2790 2795 2802 rVB 164328 331109 13.13% 2.496% 10 33.682 3113 3119 3135 rBV2 550827 1256949 49.85% 9.477%

11 33.903 3138 3143 3153 rVB 22314 51549 2.04% 0.389% 12 37.924 3574 3581 3596 rBV2 256577 785138 31.14% 5.920%

Sum of corrected areas: 13263026

5750 .D GCMS0408.M Tue Apr 16 08:15:50 2002

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