GCMS blank analysis results for sample AE05847, April 16 2002

NYC 9/11 Public Portal Document

Quantitation ort (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0302\q .D Vial: 2 Acq On 4 Apr 2002 3:31 am gP Operator: Sample Inst : MS 209 Mise Multiplr: 0 MS Integration Params: GOOFY.P Quant Time: Apr 4 8:32 2002 Quant Results File: GCMS0403.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 03 15:44:21 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 660756 20.00 ug/1 ■ 0.00 10) Naphthalene-d8 15.89 136 2446580 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.20 164 1420033 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.64 188 2143058 20.00 ug/1 -0.02 38) Chrysene-dl2 33.71 240 1210076 20.00 ug/1 0.00 44) Perylene-dl2 37.94 264 638931 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 5^ Qvalue 2) N-nitroso-dimethyl amine 5.90 74 742182 83.09 ug/1 99 3) bis(2-Chloroethyl)ether 11.67 93 1155322 79.71 ug/1 98 4) 1,3-Dichlorobenzene 12.15 146 1289430 83.37 ug/l 99 5) 1,4-Dichlorobenzene 12.30 146 1295891 . 83.32 ug/1 100 6) 1,2-Dichlorobenzene 12.81 146 1205753 82.89 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.14 45 1561954 80.58 ug/1 99 8) N-Nitroso-di-n-propylamine 13.54 70 760411 82.91 ug/1 100 9) Hexachloroethane 13.66 117 471953 83.44 ug/1 99 11) Nitrobenzene 13.94 77 1131357 81.98 ug/1 99 12) Isophorone 14.60 82 2141837 83.32 ug/1 100 13) bis(2-Chloroethoxy)methane 15.28 93 1421516 83.11 ug/1 99 14) 1,2,4-Trichlorobenzene 15.78 180 1073828 84.24 ug/1 100 15) Naphthalene 15.95 128 3255694 83.58 ug/1 100 16) Hexachlorobutadiene 16.49 225 551385 85.04 ug/1 100 18) Hexachlorocyclopentadiene 18.68 237 391524 85.70 ug/1 99 19) 2-Chloronaphthalene 19.46 162 2032983 82.31 ug/1 100 20) Dimethylphthalate 20.55 163 2363000 82.80 ug/1 100 21) 2,6-Dinitrotoluene 20.77 165 570277 84.71 ug/1 99 22) Acenaphthylene 20.73 152 2876186 83.57 ug/1 100 2 3) Acenaphthene 21.30 153 2029798 82.96 ug/1 100 24) 2,4-Dinitrotoluene 21.94 165 737185 85.51 ug/1 99 25) Diethylphthalate 22.69 149 2250920 83.91 ug/1 99 26) 4-Chlorophenyl-phenylether 22.83 204 1034994 83.29 ug/1 100 27) Fluorene 22.82 166 2177830 83.66 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 2164768 81.62 ug/L 98 30) N-Nitrosodiphenylamine 23.23 168 955578 82.01 ug/1 100 31) 4-Bromophenyl-phenylether 24.30 248 585225 83.07 ug/1 98 32) Hexachlorobenzene 24.74 284 693063 82.24 ug/1 100 33) Phenanthrene 25.71 178 3004162 82.30 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0408.M Tue Apr 16 07:59:32 2002 Page 1

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