GCMS sample AE05056 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5055.D Vial: 31 Acq On : 30 Mar 2002 10:42 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.31 ug/1 36371 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW .MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1-Hexanol, /6-amino- 117 C6H15NO 004048-33-3 9 3 2-Methyl-5Ahexen-3-ol 114 C7H14O 032815-70-6 9 4 Methane, d/sothiocyanato- 73 C2H3NS __ __ 000556-61-6 4 Abundance ' " f . Scan 337 (87w^^ Tb

5000 43

,x,jJ,1,4.9 55 87 103 7.80 8.00 8.20 8.40 ' I ' ' ‘ 'I 1 ' ' ' I m/ z 42.95 26.91% m/z->.. ....... 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

I 5000 58 7.80__ 8.00 8.20 8.40 44 !

’m/z-> Abundance I ' ' 10 15 ' ‘ I 20 u 30 40 ,|.i , 50 60 -04393:1-Hsxanol, S-aniino- 70 80 90 100 110 m/z 41.0,5 9.59%

30 JU JU __L80_jB:00_J,20__a40_^^ 5000 m/z 44.95 8.80%

........ . .............. ............................. , , , , !m/z-> 10__ 20__ 30__ 40___ 50 60 70 SO 90 ' l66 ' 'l10 Abundance #3017: 2-Methyi-5-hexen-3-oi ...... 70 _JL8O_8,OO__82O__J4^^ 55 m/z 71.0,0 6.40% 43 5000

I i 27 I , JU. J,..... I 81 'm/z-> 10 20 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5055.D GCMS0308.M Tue Apr 02 15:33:17 2002 Page 1 ■

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