GCMS analysis results sample AE04595, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\4595.D Vial: 11 Acq On : 26 Mar 2002 7:37 pm Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title :• 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 2.06 ug/1 415948 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethyl^rmamide 73 C3H7NO 000627-45-2 9 2 3-Pent^ol, 3-methyl- 102 C6H14O 000077-74-7 9 3 1,3-D^xolane, 2- (3-bromo-5,5,5-tri 352 C10H16BrC13O2 0'00000-00-0 9 4 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 Abundance Scan 337 (8.136 mln): 45^ (-} m/ z 73.0 0. “To 6."^ 713

5000 43 .............. , ....... 37, 1,1 I 55 __ 7^ 8.00 8.20 8.40 , 67, I I 103 ' I ' ' ' ' I ' ' ' 'I' I'. , I , ' I ' ' ‘ 'I' m/z 4’3~0.5' ’ 28.13% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 3l0 73

5000 44 58 7,80__ 8,00 8.20 8.4^____ "m/r 4 5 ■ id.23% 15

iTl/z->10 20 30___ 40___ 50___ 60___ 70__ 80___ 90__ 100 110 120 Abundance #63573 3-Pent3rio!. d-inetuyi- 73

7.80 -8:00 _ 5 20 8.40 m/ z

IZj 5000

55 45 87 27 39 ' I ' ' ' ' I ' ' ' ' I ' ' I ' ' ' 'm/z~> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 7.80 8.00 8.20 8.40 __ m/ z 71.00 6.67% 5000 1 45 36 ,|| 55 67 109 115 ! 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

4595.D GCMS0308.M Thu Mar 28 16:30:39 2002 Page 1

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