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GCMS analysis page, sample AE01153, March 2002

Machine-extracted title · confidence 100%

Laboratory report page showing surrogate recovery data for sample AE01153 analyzed on March 22, 2002.

NYC-WTC_000058798–000058815

Folder label: “GCMS X 3/7/02 A 3/27/02

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Scanned page image, NYC-WTC_000058805
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\FEB1502\1153.D Vial: 7 Acq On 15 Feb 2002 9:18 pm Operator: 209 GALOS Sample gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M .(RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.31 ug/1 43017 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 36 2 Pentane/ 3-methoxy- 102 C6H14O 036839-67-5 9 3 N-Ethyl/formamide 73 C3H7NO 000627-45-2 5 5-2-(3-Mpthyl-3-nitrobutyl)-1,3-dioxo 189 C8H15NO4 057620-56-1 4 'Abundance Scan 345 (8.208 min); 1153.D (-) 713 m/z. “ vy/oo 100 .“oo%

5000 43 ...........

I, 49,,.55 87' 103 7-80 8.00 8.20 8.40 8.60 . ... ...... m/z 43.05 37.59%

jX m/Z;->......... . 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 713

5000 7.80 8.00 8.20 8.40 8.60 55 m/z 40.95 13.54% 45 87 27 1, .... , , ,1 ' 39, I , , I ’m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance ' . #1793: Pentane, S-methoxy- 1 73 '' ' I ’ 7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 12.97% 45

33 39 55 'm/z-> Abundance 10 20 30

30 40L____ .50 . . .. 60____ 70_____ 80_____ 90____ WO____ 110 #292: N-Ethylformamide

73 7.80 m/z 8.00 Ju 8.20 39.05 8.40 8.60 6.69% 5000 44 58

15 I ' ' ' ' I 10 20 4 30 40 50 60 70 80 90 100 110 7.80 8.00 A, 8.20 8.40 8.60

1153 .D GCMS0208 .M Fri Mar 08 15:16:08 2002 Page 1

NYC-WTC_000058805

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NYC-WTC_000058805Source: NYC Law Department, mirrored locally

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