GCMS chromatogram data for sample AE04592, April 2002

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Data File : C:\HPCHEM\1\DATA\MAR26O2\4592.D Vial: 8 Acq On : 26 Mar 2002 4:38 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GGMS0308.M (RTE Integrator) ■ Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.95 2.03 ug/1 260547 Chrysene-dl2 33.70

Hit# of 5 Tent^ive ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 1-Monolinolec^lglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 23 3 Benzoic acid/ 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 14 4 Noradrenaline, tetra-TMS 457 C20H43Nq3Si4 000000-00-0 14 Abundance .. Scan"3257 m/z .. 7|3

147 5000 221 281 355

45 117 , 191 [ 251, 1 L 429 34.60 34.80 35.00 35.20 m/z 147. 53.87% m/z--> 50 100 150 200 250 300 350 400 450 Abundance #56714: 1,1,i,57,7,7-Heptamelhyl-3,3-bis(frimethylsiioxyjt 70 147 5000 267 , 355 429 __34.6O_ 3<80_ 35.00 35.20 ___ 207 m/z 221“. 0,5 43.80% I !

'm/z--> '*5 i 50 100 150 200 I 250 ..Il... !,i, 300 350 400 450 Abundance #53871; 1-Monoiinol£»yiglycoroi tri-netiiyisilyl ether 73

207 34.60 34.80 35.00 35.20 5000 147 m/z 355.0,5 30.45% 34 103 I 281 395 482 mfe-> 50 100 150 -200___ 250 300 350___ 400 450 Abundance #51296: Benzoic acid, 2.6-bis[(trimethylsilyl)oxy]-. trimet 713 ■ 355 34.60 34.80 35.00 35.20 m/z 281.0,5 26.70% 5000 I

147 267 47 208 237, J m/z-> 50 1PO 15P 200 250 300 350 400 450 34.60 34.80 35.00 35.20

4592.D GCMS0308.M Thu Mar 28 16:27:57 2002 Page 2

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