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Pesticide residue analysis results, sample AD28043, Jan 2002

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Lab analysis of sample AD28043 for pesticide and chemical residues, all results below method detection limits, completed Jan 29, 2002.

NYC-WTC_000058147–000058152

Folder label: “525 X 1/11/02 A 1/26/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\28043.D Vial: 11 ^cq On Sample Mise : 10 Dec 2001 : sample : 11:54 pm Operator: Inst Multiplr: : McLean Instrumen 1.00 Jetyla MS Integration Params: BENZO.P Quant Time: Dec 11 00:31:39 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.44 164 141697 5.00 ug/L 0.13 9) Phenanthrene D-10 22.80 188 24122 5.00 ug/L 0.16 20) Chrysene D-12 30.56 240 81288 5.00 ug/L 0.14

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.36 134 5022 0.67 ug/L 0.14 Spiked Amount 5.000 Recovery 13.40% 19) Triphenyl Phosphate surr 29.75 326 62350 74.56 ug/L 0.06 Spiked Amount 5.000 Recovery = 1491.20% 21) Perylene D-12 surr 34.54 264 58078 5.09 ug/L 0.10 Spiked Amount 5.000 Recovery = 101.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 18.44 165 13959 2.70 ug/L # 30 7) 2,4-Dinitotoluene 19.06 165 1221 0.47 ug/L # 21 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. 18) 4,4'-DDE 0.00 246 0 N.D. 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D 23) Bis (2-Ethylhexyl) phthala 31.08 149 17174 n 78 24) Benzo (a) pyrene 0.00 252 0

s

(#) = qualifier out of range (m) = m< 28043.D 012402B.M Mon Jan 28 15 Page 1

NYC-WTC_000058150

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NYC-WTC_000058150Source: NYC Law Department, mirrored locally

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