Pesticide analysis results, sample AD27390, Nov-Dec 2001

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27390.D Vial: 20 cq On 7 Dec 2001 6:55 am Operator: McLean Sample 11/19 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 14:31:18 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Wed Dec 12 12:56:58 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6921233 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 10324394 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 7496727 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1425181 3.88 ug/L 0.00 Spiked Amount 5.000 Recovery = 77.60% 19) Triphenyl Phosphate surr 29.70 326 2287984 6.39 ug/L 0.00 Spiked Amount 5.000 Recovery = 127.80% 21) Perylene D-12 surr 34.44 264 4706087 4.47 ug/L 0.00 Spiked Amount 5.000 Recovery = 89.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.51 284 7413 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.93 165 96263 0.58 ug/L # 36 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.23 126 6306 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 17043 0.12 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.06 149 1179910 0.78 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27390.D 120501.M Wed Dec 12 14:33:26 2001 Page 1

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