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Sample analysis results, sample AD27491, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27491 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055150–000055153

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27491.D Vial: 21 . Acq On 7 Dec 2001 7:40 am Operator: McLean Sample 11/19 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 07 08:17:40 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6573028 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 10146860 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 7248552 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1450053 4.16 ug/L 0.00 Spiked Amount 5,000 Recovery = 83.20% 19) Triphenyl Phosphate surr 29.70 326 2166336 6.16 ug/L 0.01 Spiked Amount 5.000 Recovery = 123.20% 21) Perylene D-12 surr 34.44 264 4976311 4.89 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.05 165 14753 0.33 ug/L # 42 8) Molinate 19.23 126 5315 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.93 162 7244 0.01 ug/L # 38 17) Butachlor 26.76 160 46854 0.11 ug/L # 9 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 28070 0.13 ug/L # 28 23) Bis (2-Ethylhexyl) phthala 31.07 149 1224308 0.83 ug/L 99 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27491.D 5080102.M Thu Jan 10 08:55:28 2002 Page 1

NYC-WTC_000055151

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NYC-WTC_000055151Source: NYC Law Department, mirrored locally

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