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Sample AD28164 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28164 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055469–000055474

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\28164.D Vial: 22 Acq On : 11 Dec 2001 7:57 am Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 08:34:41 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.34 164 1077126 5.00 ug/L 0.03 9) Phenanthrene D-10 22.66 188 9108735 5.00 ug/L 0.02 20) Chrysene D-12 30.44 240 6110372 5.00 ug/L 0.02

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1468547 25.69 ug/L 0.02 Spiked Amount 5.000 Recovery = 513.80% 19) Triphenyl Phosphate surr 29.70 326 2045144 6.48 ug/L 0.00 Spiked Amount 5,000 Recovery = 129.60% 21) Perylene D-12 surr 34.48 264 1282611 1.50 ug/L 0.04 Spiked Amount 5.000 Recovery 30.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.52 284 5435 0.07 ug/L # 67 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.27 165 4281 0.37 ug/L 84 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 26.78 160 21551 0.06 ug/L # 13 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 14999 0.12 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 117003 0.24 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 28164.D 120501.M Thu Jan 10 12:13:58 2002 Page 1

NYC-WTC_000055470

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NYC-WTC_000055470Source: NYC Law Department, mirrored locally

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