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Sample AD28166 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28166 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055475–000055480

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\28166.D Vial: 23 Acq On : 11 Dec 2001 8:42 am Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 14:11:10 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6649733 5.00 ug/L 0.00 9) Phenanthrene D-10 22.66 188 10254163 5.00 ug/L 0.02 20) Chrysene D-12 30.43 240 6427829 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1519893 4.31 ug/L 0.02 Spiked Amount 5.000 Recovery = 86.20% 19) Triphenyl Phosphate surr 29.70 326 2207223 6.21 ug/L 0.00 Spiked Amount 5.000 Recovery = 124.20% 21) Perylene D-12 surr 34.45 264 3659403 4.06 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachiorobenzene 21.52 284 7304 0.01 ug/L # 75 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. d 10) Simazine 22.10 201 6771 0.02 ug/L # 18 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 24.23 146 10117 0.04 ug/L # 79 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 25.38 162 5826 0.01 ug/L 67 17) Butachlor 26.58 160 6473 0.02 ug/L 92 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 42690 0.15 ug/L # 21 23) Bis (2-Ethylhexyl) phthala 31.07 149 429709 0.43 ug/L 90 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28166.D 120501.M Thu Jan 10 12:14:41 2002 Page 1

NYC-WTC_000055476

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NYC-WTC_000055476Source: NYC Law Department, mirrored locally

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