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Sample AD28045 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28045 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055433–000055438

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\28045.D Vial: 13 Acq C ■> : 11 Dec 2001 1:24 am Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 02:01:21 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 5925051 5.00 ug/L 0.00 9) Phenanthrene D-10 22.66 188 9905210 5.00 ug/L 0.02 20) Chrysene D-12 30.43 240 5998672 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1066371 3.39 ug/L 0.02 Spiked Amount 5.000 Recovery = 67.80% 19) Triphenyl Phosphate surr 29.70 326 2026976 5.90 ug/L 0.00 Spiked Amount 5.000 Recovery = 118.00% 21) Perylene D-12 surr 34.46 264 3793706 4.51 ug/L 0.02 Spiked Amount 5.000 Recovery = 90.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.94 165 112467 0.71 ug/L # 35 7) 2,4-Dinitotoluene 19.16 165 6735 0.31 ug/L 82 8) Molinate 19.24 126 5158 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.66 161 95009 0.22 ug/L # l 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.92 162 5286 0.00 ug/L # 38 17) Butachlor 26.77 160 47337 0.12 ug/L # 10 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 18933 0.13 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 219990 0.31 ug/L 97 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28045.D 120501.M Thu Jan 10 12:05:33 2002 Page 1

NYC-WTC_000055434

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NYC-WTC_000055434Source: NYC Law Department, mirrored locally

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