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Sample AD27986 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD27986 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055421–000055426

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\27986.D Vial: 10 Acq On : 10 Dec 2001 11:09 pm Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 10 23:46:47 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6312096 5.00 ug/L 0.00 9) Phenanthrene D-10 22.66 188 9380508 5.00 ug/L 0.02 20) Chrysene D-12 30.43 240 5958134 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1366773 4.08 ug/L 0.02 Spiked Amount 5.000 Recovery = 81.60% 19) Triphenyl Phosphate surr 29.70 326 1948312 5.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.80% 21) Perylene D-12 surr 34.45 264 3781102 4.52 ug/L 0.00 Spiked Amount 5.000 Recovery = 90.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 12 8 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.25 126 11739 0.01 ug/L # l 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 23.69 146 6377 0.03 ug/L # 73 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 26.76 160 44740 0.12 ug/L # 9 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.61 129 30631 0.14 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 228223 0.32 ug/L 94 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27986.D 120501.M Thu Jan 10 12:00:03 2002 Page 1

NYC-WTC_000055422

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NYC-WTC_000055422Source: NYC Law Department, mirrored locally

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