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Pesticide analysis results, sample AD27391, Nov-Dec 2001

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Laboratory report showing non-detect results for pesticides and organic contaminants in sample AD27391.

NYC-WTC_000057136–000057139
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27391.D Vial: 44 q fn 8 Dec 2001 1:34 am Operator: McLean Sample 11/15 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 14:32:14 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Wed Dec 12 12:56:58 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.32 164 5681149 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 9436010 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 6052827 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1316083 4.36 ug/L 0.00 Spiked Amount 5.000 Recovery = 87.20% 19) Triphenyl Phosphate surr 29.70 326 1879882 5.75 ug/L 0.01 Spiked Amount 5.000 Recovery = 115.00% 21) Perylene D-12 surr 34.45 264 3359174 3.95 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.05 165 18765 0.35 ug/L # 21 8) Molinate 19.25 126 9854 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 24.20 146 6174 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.93 162 5517 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 35880 0.15 ug/L # 26 23) Bis (2-Ethylhexyl) phthala 31.07 149 578935 0.54 ug/L 92 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27391.D 120501.M Wed Dec 12 14:32:58 2001 Page 1

NYC-WTC_000057137

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NYC-WTC_000057137Source: NYC Law Department, mirrored locally

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