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Sample analysis results, sample AD27547, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27547 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055115–000055118

Folder label: “525 X 11/16/01 A 12/5/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120501\25747.D Vial: 11 7 On 5 Dec 2001 10:48 pm Operator: McLean £ ample sample 11/16 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 09:37:03 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.31 164 7160716 5.00 ug/D 0.00 9) Phenanthrene D-10 22.64 188 10629845 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 7587959 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1581398 4.16 ug/L 0.00 Spiked Amount 5.000 Recovery = 83.20% 19) Triphenyl Phosphate surr 29.69 326 2200889 5.97 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.40% 21) Perylene D-12 surr 34.43 264 4525859 4.25 ug/L 0.00 Spiked Amount 5.000 Recovery = 85.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.50 284 12107 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.05 165 20319 . 0.34 ug/L # 29 8) Molinate 19.24 126 7555 C N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 24.11 160 5537 N.D. 13) Terbacil 23.20 161 5685 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.40 246 7836 N.D. 22) Bis (2-Ethylhexyl) adipate 29.62 129 40124 0.14 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.06 149 301744 0.32 ug/L 96 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 25747.D 120501.M Tue Dec 11 09:38:03 2001 Page 1

NYC-WTC_000055116

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NYC-WTC_000055116Source: NYC Law Department, mirrored locally

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