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Pesticide and contaminant analysis results, Nov-Dec 2001

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Laboratory report showing non-detect results for various pesticides and organic contaminants in sample AD27274.

NYC-WTC_000057073–000057076
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\120601\27275.D Vial: 41 Acq On 7 Dec 2001 11:19 pm Operator: McLean Sample 11/15 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 14:21:22 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Wed Dec 12 12:56:58 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.32 164 5044823 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 8235327 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 5342836 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 978539 3.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 73.00% 19) Triphenyl Phosphate surr 29.70 326 1789523 6.27 ug/L 0.00 Spiked Amount 5.000 Recovery = 125.40% 21) Perylene D-12 surr 34.45 264 3377515 4.50 ug/L 0.00 Spiked Amount 5.000 Recovery = 90.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.05 165 4280 0.30 ug/L # 47 8) Molinate 19.08 126 10517 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.75 161 6201 N.D. 14) Acetochlor 23.96 146 5455 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.65 162 6361 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 20784 0.13 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 323949 0.41 ug/L 99 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27275.D 120501.M Wed Dec 12 14:22:08 2001 Page 1

NYC-WTC_000057074

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NYC-WTC_000057074Source: NYC Law Department, mirrored locally

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