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Pesticide and contaminant analysis results, Nov-Dec 2001

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Laboratory report listing quantitative results for pesticides and organic contaminants in sample AD27232.

NYC-WTC_000057061–000057064
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\120601\27232.D Vial: 43 Acq On 8 Dec 2001 12:49 am Operator: McLean Sample 11/15 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 13:06:07 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Wed Dec 12 12:56:58 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 5059275 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 8469639 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 5107972 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 991586 3.69 ug/L 0.00 Spiked Amount 5.000 Recovery = 73.80% 19) Triphenyl Phosphate surr 29.70 326 1716121 5.84 ug/L 0.00 Spiked Amount 5.000 Recovery = 116.80% 21) Perylene D-12 surr 34.45 264 3073996 4.29 ug/L 0.00 Spiked Amount 5.000 Recovery = 85.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.08 126 8553 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 25.28 162 5515 N.D. 17) Butachlor 26.76 160 32418 0.09 ug/L # 4 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 22615 0.14 ug/L # 14 23) Bis (2-Ethylhexyl) phthala 31.07 149 462726 0.52 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27232.D 120501.M Wed Dec 12 14:20:15 2001 Page 1

NYC-WTC_000057062

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NYC-WTC_000057062Source: NYC Law Department, mirrored locally

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