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Sample analysis results, sample AD27544, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27544 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055158–000055161

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27544.D Vial: 22 Acq On 7 Dec 2001 8:25 am Operator: McLean Sample 11/19 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 07 09:02:39 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.32 164 6700106 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 10681442 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 7022739 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1495617 4.21 ug/L 0.00 Spiked Amount 5.000 Recovery = 84.20% 19) Triphenyl Phosphate surr 29.70 326 2158853 5.83 ug/L 0.00 Spiked Amount 5.000 Recovery = 116.60% 21) Perylene D-12 surr 34.44 264 4604474 4.67 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.52 284 9947 0.02 ug/L 88 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.06 165 15147 0.33 ug/L # 32 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 26.76 160 48699 0.11 ug/L # 6 18) 4,4'-DDE 27.40 246 8723 0.02 ug/L 83 22) Bis (2-Ethylhexyl) adipate 29.62 129 44992 0.15 ug/L # 34 23) Bis (2-Ethylhexyl) phthala 31.06 149 4722163 2.67 ug/L 100 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27544.D 5080102.M Thu Jan 10 08:46:48 2002 Page 1

NYC-WTC_000055159

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NYC-WTC_000055159Source: NYC Law Department, mirrored locally

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