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Sample analysis results, sample AD27548, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27548 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055170–000055173

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27548.D Vial: 23 Acq On 7 Dec 2001 9:10 am Operator: McLean Sample 11/19 sample Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 07 09:47:31 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6859667 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 9745229 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 6532536 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1414564 3.88 ug/L 0.00 Spiked Amount 5.000 Recovery = 77.60% 19) Triphenyl Phosphate surr 29.69 326 2090145 6.19 ug/L 0.00 Spiked Amount 5,000 Recovery = 123.80% 21) Perylene D-12 surr 34.44 264 4012743 4.38 ug/L 0.00 Spiked Amount 5.000 Recovery = 87.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.51 284 12289 0.02 ug/L # 76 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.93 165 182964 0.91 ug/L # 36 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.23 126 6694 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 23.98 160 5647 0.02 ug/L # 1 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 30128 0.14 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.06 149 1904838 1.29 ug/L 96 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27548.D 5080102.M Thu Jan 10 08:49:23 2002 Page 1

NYC-WTC_000055171

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NYC-WTC_000055171Source: NYC Law Department, mirrored locally

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