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Sample AD27984 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD27984 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055409–000055414

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\27984.D Vial: 8 Acq On : 10 Dec 2001 9:39 pm Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 10 22:17:02 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.32 164 6239087 5.00 ug/L 0.00 9) Phenanthrene D-10 22.66 188 9823940 5.00 ug/L 0.02 20) Chrysene D-12 30.44 240 5430888 5.00 ug/L 0.02

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1245913 3.76 ug/L 0.02 Spiked Amount 5.000 Recovery = 75.20% 19) Triphenyl Phosphate surr 29.70 326 1800736 5.29 ug/L 0.00 Spiked Amount 5.000 Recovery = 105.80% 21) Perylene D-12 surr 34.46 264 3432643 4.50 ug/L 0.02 Spiked Amount 5.000 Recovery = 90.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.53 284 5875 0.01 ug/L # 67 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.66 165 10992 0.32 ug/L 98 8) Molinate 19.24 126 6269 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.81 161 5945 0.01 ug/L # 1 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 11694 0.12 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 263727 0.36 ug/L 100 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27984.D 120501.M Thu Jan 10 11:58:17 2002 Page 1

NYC-WTC_000055410

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NYC-WTC_000055410Source: NYC Law Department, mirrored locally

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