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Sample AD27985 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD27985 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055415–000055420

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121001B\27985.D Vial: 9 Acq On : 10 Dec 2001 10:24 pm Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 10 23:01:54 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.33 164 6089049 5.00 ug/L 0.02 9) Phenanthrene D-10 22.66 188 9157752 5.00 ug/L 0.02 20) Chrysene D-12 30.43 240 5517762 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 1147040 3.55 ug/L 0.02 Spiked Amount 5.000 Recovery = 71.00% 19) Triphenyl Phosphate surr 29.70 326 1962464 6.18 ug/L 0.00 Spiked Amount 5.000 Recovery = 123.60% 21) Perylene D-12 surr 34.45 264 3837069 4.95 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 .0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.25 126 5172 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.94 162 5361 0.01 ug/L # 38 17) Butachlor 26.77 160 40593 0.11 ug/L # 3 18) 4,4'-DDE 27.53 246 493857 1.30 ug/L # 23 22) Bis (2-Ethylhexyl) adipate 29.61 129 13933 0.13 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 207263 0.32 ug/L 99 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27985.D 120501.M Thu Jan 10 11:58:50 2002 Page 1

NYC-WTC_000055416

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NYC-WTC_000055416Source: NYC Law Department, mirrored locally

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