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Water sample analysis results, sample AD27395, Nov-Dec 2001

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Laboratory report listing analytical results for pesticides and organic compounds in water sample AD27395.

NYC-WTC_000057758–000057761

Folder label: “525 11/15/01 12/6 - 12/7 12/4 - 12/5 TWO INSTR.

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

. Data File : C:\MSDCHEM\1\DATA\120501\27395.D Vial: 16 eq on : 6 Dec 2001 2:33 am Operator: McLean Sample : sample 11/16 Inst : Instrumen Mise : Multiple: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 09:43:47 2001 Quant Results File: 120501.RES Quant Method : C:\MSDCHEM\1\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) Acenaphthene-d10 18.31 164 6152736 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 9322175 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 6405089 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3 -Dimethyl - 2 -nitrobenzen 13.23 134 1286244 3.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 78.80% 19) Triphenyl Phosphate surr 29.69 326 1840265 5.69 ug/L 0.00 Spiked Amount 5.000 Recovery = 113.80% 21) Perylene D-12 surr 34.44 264 4130760 4.59 ug/L : 0.00 Spiked Amount 5.000 Recovery = 91.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 12 8 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.06 165 10746 0.32 ug/L # 38 8) Molinate 19.25 126 7770 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d O 22) Bis (2-Ethylhexyl) adipate 29.62 129 23399 0.13 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.06 149 430574 0.43 ug/L 98 • 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual 'integration 27395.D 120501.M Tue Dee 11 09:44:45 2001 Page 1

NYC-WTC_000057759

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NYC-WTC_000057759Source: NYC Law Department, mirrored locally

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