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Water sample analysis results, sample AD27394, Nov-Dec 2001

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Laboratory report listing analytical results for pesticides and organic compounds in water sample AD27394.

NYC-WTC_000057754–000057757

Folder label: “525 11/15/01 12/6 - 12/7 12/4 - 12/5 TWO INSTR.

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\120501\27394 .D Vial: 15 Acq n : 6 Dec 2001 1:48 am Operator: McLean Sample : sample 11/16 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 09:42:26 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\1\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.31 164 5552844 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 7967819 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 5628516 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3 -Dimethyl -2 -nitrobenzen 13.23 134 1125661 3.82 ug/L 0.00 Spiked Amount 5.000 Recovery 76.40% 19) Triphenyl Phosphate surr 29.69 326 1765847 6.39 ug/L 0.00 Spiked Amount 5.000 Recovery = 127.80% 21) Perylene D-12 surr 34.44 264 3160746 4.00 ug/L 0.00 Spiked Amount 5.000 Recovery = 80.00%

Target compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 12 8 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.25 165 8172 0.31 ug/L 74 8) Molinate 19.24 126 9301 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. ) 13) Terbacil 22.93 161 5661 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 ■ 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.61 129 23871 0.14 ug/L # 8 23) Bis (2-Ethylhexyl) phthala 24) Benzo (a) pyrene 31.06 0.00 149 252 316837 0 0.39 ug/L N.D. d 95 <0 0

(#) = qualifier out of range (m) = manual integration 27394.D 120501.M Tue Dec 11 09:43:36 2001 Page 1

NYC-WTC_000057755

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NYC-WTC_000057755Source: NYC Law Department, mirrored locally

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