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Sample AD28106 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28106 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055463–000055468

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

ops Data File : C:\MSDCHEM\1\DATA\121001B\28106.D Vial: 21 Acq On : 11 Dec 2001 7:12 am Operator: McLean Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 07:49:49 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.33 164 5170340 5.00 ug/L 0.02 9) Phenanthrene D-10 22.66 188 8256715 5.00 ug/L 0.02 20) Chrysene D-12 30.43 240 5168786 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.24 134 980939 3.57 ug/L 0.02 Spiked Amount 5.000 Recovery = 71.40% 19) Triphenyl Phosphate surr 29.70 326 1677008 5.86 ug/L 0.00 Spiked Amount 5.000 Recovery = 117.20% 21) Perylene D-12 surr 34.46 264 3325250 4.58 ug/L 0.02 Spiked Amount 5.000 Recovery = 91.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.37 165 5451 0.31 ug/L 74 8) Molinate 19.24 126 6826 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 24.01 146 8036 0.04 ug/L 94 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 30823 0.15 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 160985 0.29 ug/L 95 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28106.D 120501.M Thu Jan 10 12:11:28 2002 Page 1

NYC-WTC_000055464

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NYC-WTC_000055464Source: NYC Law Department, mirrored locally

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