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Sample analysis results, sample AD27492, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27492 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055154–000055157

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\120601\27492.D Vial: 34 * Acq On 7 Dec 2001 6:04 pm Operator: McLean Sample ll/19sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 07 18:41:52 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6896057 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 9879044 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 6304803 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1362306 3.72 ug/L 0.00 Spiked Amount 5.000 Recovery = 74.40% 19) Triphenyl Phosphate surr 29.70 326 2211330 6.46 ug/L 0.00 Spiked Amount 5.000 Recovery = 129.20% 21) Perylene D-12 surr 34.44 264 4415536 4.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.93 165 172198 0.87 ug/L # 34 7) 2,4-Dinitotoluene 19.06 165 20698 0.35 ug/L # 31 8) Molinate 0.00 126 0 N.D. d 10) Simazine 22.04 201 7174 0.03 ug/L 96 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 23.57 160 6255 0.02 ug/L # 1 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 23.63 146 6041 0.02 ug/L 97 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 26.76 160 45179 0.11 ug/L # 8 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 28006 0.14 ug/L # 11 23) Bis (2-Ethylhexyl) phthala 31.07 149 1482574 1.08 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27492.D 5080102.M Thu Jan 10 08:46:13 2002 Page 1

NYC-WTC_000055155

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NYC-WTC_000055155Source: NYC Law Department, mirrored locally

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