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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09585 Sample Date/Time: Tuesday, May 14, 2002 10:09:34 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:wwinnt\profiles\rd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09585.017 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 12.667 19.868 0.000' 0.00865 63.98 ug/L > Sc-1 45 582694.069 1.099 582694.069 ug/L Cr 52 11314.817 0.774 0.004 0.20387 4.79 ug/L Cr 53 2473.695 3.008 0.003 1.10408 4.95 ug/L Mn 55 366150.058 1.938 0.627 17.45748 2.98 ug/L Ni 60 1737.850 1.907 0.003 0.55108 1.64 ug/L Cu 63 9010.226 4.600 0.015 1.31972 5.26 ug/L Cu 65 4207.351 5.271 0.007 1.28378 5.61 ug/L Zn 66 2909.495 2.457 0.015 0.87905 5.65 ug/L Zn 67 692.700 3.984 0.004 1.32135 3.66 ug/L Zn 68 2910.829 4.366 0.017 1.32607 4.53 ug/L Ge 72 127437.043 1.415 127437.043 ug/L As 75 6932.232 1.610 0.010 0.47840 2.21 ug/L Se 77 971.611 4.196 0.001 0.56855 19.65 ug/L Se 82 57.408 3.273 0.001 0.24829 1.49 ug/L Kr 83 2255.302 0.626 -249.401 ug/L Ag 107 221.005 10.006 -0.000 -0.00772 20.46 ug/L > In 115 1671455.561 0.369 1671455.561 ug/L Sb 121 658.697 3.529 0.000 0.06069 3.42 ug/L Sb 123 516.081 1.272 0.000 0.06183 1.74 ug/L Ba 135 53541.406 0.364 0.020 15.58973 1.38 ug/L Ba 137 93422.913 1.524 0.035 15.46559 1.13 ug/L > Tb 159 2668124.891 1.520 2668124.891 ug/L Hg 201 60.001 10.000 0.000 0.00845 44.98 ug/L Hg 202 121.669 10.342 0.000 0.00699 54.61 ug/L TI 205 1059.406 4.851 0.000 0.00273 51.79 ug/L Pb 208 6796.393 1.589 0.001 0.07794 0.16 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 82.687 Cr 52 Cr 53 Mn 55

Sample ID: AE09585 Report Date/Time: Tuesday, May 14, 2002 10:11:15 Page 1

NYC-WTC_000053422

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