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ICPMS daily performance check report, May 14, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09577 Sample Date/Time: Tuesday, May 14, 2002 09:53:20 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09577.012 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 24680.706 1.068 0.042' 51.55903 2.92 ug/L Se-1 45 582736.743 2.122 582736.743 ug/L Cr 52 623839.609 3.004 1.055 49.37000 0.97 ug/L Cr 53 76617.948 0.528 0.130 51.25989 1.66 ug/L Mn 55 1478503.716 1.973 2.535 70.64056 0.57 ug/L Ni 60 158355.447 1.664 0.272 51.28605 0.93 ug/L Cu 63 382835.221 1.217 0.657 58.08384 1.80 ug/L Cu 65 185158.032 1.521 0.317 58.68552 0.79 ug/L Zn 66 120547.956 1.427 0.925 54.50344 2.13 ug/L Zn 67 21038.198 1.963 0.161 54.12412 0.97 ug/L Zn 68 91319.310 1.100 0.700 55.34910 0.66 ug/L Ge 72 129256.099 1.123 129256.099 ug/L As 75 144437.005 0.252 1.073 52.32703 1.36 ug/L Se 77 14841.709 0.329 0.108 56.90626 1.14 ug/L Se 82 16228.648 1.102 0.126 55.52556 0.95 ug/L Kr 83 2318.319 2.538 -186.385 ug/L Ag 107 664145.195 0.898 0.393 45.70212 1.55 ug/L > In 115 1690907.453 0.922 1690907.453 ug/L Sb 121 572702.165 0.663 0.339 54.80023 0.79 ug/L Sb 123 441022.997 1.436 0.261 55.50719 1.62 ug/L Ba 135 220999.346 1.029 0.083 64.17463 1.56 ug/L Ba 137 387273.279 0.709 0.145 63.94066 0.90 ug/L > Tb 159 2677351.076 1.412 2677351.076 ug/L Hg 201 6735.562 0.631 0.002 4.01413 0.84 ug/L Hg 202 15387.500 0.967 0.006 4.01742 0.79 ug/L U 205 1757415.820 2.077 0.656 43.62227 0.95 ug/L Pb 208 2367406.798 0.407 0.883 47.34036 1.20 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff ' Be 9 103.118 > Sc-1 45 82.693 Cr 52 98.549 Cr 53 101.168 Mn 55 100.690

Sample ID: AE09577 Report Date/Time: Tuesday, May 14, 2002 09:55:42 Page 1

NYC-WTC_000053412

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