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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09517 Sample Date/Time: Wednesday, May 08, 2002 14:49:14 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09517.822 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 19377.826 1.202 0.046 57.38005 2.93 ug/L > Se-1 45 424146.006 1.770 424146.006 ug/L Cr 52 464811.588 1.079 1.080 49.24299 0.72 ug/L Cr 53 56332.300 2.605 0.131 49.80955 2.64 ug/L Mn 55 1064684.100 1.291 2.497 67.99604 0.57 ug/L Ni 60 133647.896 0.345 0.315 53.68671 1.56 ug/L Cu 63 290708.318 0.711 0.685 52.15091 2.48 ug/L Cu 65 142328.512 1.904 0.335 51.98970 3.70 ug/L Zn 66 100953.488 1.049 0.888 53.50086 0.33 ug/L Zn 67 17580.162 2.049 0.154 51.47822 1.83 ug/L Zn 68 75624.366 1.291 0.665 52.73498 1.75 ug/L > Ge 72 112935.366 1.340 112935.366 ug/L As 75 130989.377 2.162 1.070 51.66350 1.25 ug/L Se 77 13244.405 3.102 0.105 56.06295 2.23 ug/L Se 82 14470.174 1.768 0.129 57.00057 1.39 ug/L Kr 83 3688.119 2.790 -773.354 ug/L Ag 107 634555.102 0.797 0.386 45.21207 0.95 ug/L In 115 1644200.963 0.794 1644200.963 ug/L Sb 121 577841.225 1.668 0.351 51.35975 0.96 ug/L Sb 123 448086.592 0.236 0.272 52.09966 0.99 ug/L Ba 135 217808.055 1.190 0.086 58.56623 0.46 ug/L Ba 137 376366.577 1.204 0.148 57.78944 0.38 ug/L > Tb 159 2534280.624 0.824 2534280.624 ug/L Hg 201 7219.605 1.412 0.003 4.10016 1.36 ug/L Hg 202 16165.188 0.320 0.006 4.06769 0.69 ug/L TI 205 1788061.814 1.000 0.705 46.02090 1.22 ug/L Pb 208 2389642.953 0.718 0.942 46.30254 0.25 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 114.741 > Sc-1 45 82.944 Cr 52 98.343 Cr 53 98.349 Mn 55 99.692

Sample ID: AE09517 Report Date/Time: Wednesday, May 08, 2002 14:51:30 Page 1

NYC-WTC_000053185

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