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ICPMS daily performance check report, May 3, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08954 Sample Date/Time: Friday, May 03, 2002 14:32:52 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE08954.741 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 25219.868 2.617 0.057 58.97867 3.42 ug/L > Se-1 45 444330.824 0.900 444330.824 ug/L Cr 52 470136.125 2.768 1.042 50.92641 3.15 ug/L Cr 53 54219.527 3.260 0.121 50.16643 4.16 ug/L Mn 55 1016554.582 2.276 2.283 68.28163 1.75 ug/L Ni 60 114951.251 2.289 0.258 55.05693 3.17 ug/L Cu 63 237263.331 0.454 0.533 53.87509 0.48 ug/L Cu 65 122515.522 2.269 0.275 55.05192 3.08 ug/L Zn 66 85305.873 3.485 0.899 52.99653 3.96 ug/L Zn 67 15503.368 2.326 0.163 53.39179 2.43 ug/L Zn 68 65950.564 3.706 0.695 54.94611 4.12 ug/L > Ge 72 93694.626 0.500 93694.626 ug/L As 75 108211.090 2.080 1.078 53.38810 2.40 ug/L Se 77 10530.792 2.679 0.102 56.59752 3.43 ug/L Se 82 14324.088 1.542 0.124 57.89092 2.46 ug/L Ag 107 423761.077 3.213 0.343 43.30658 3.73 ug/L Cd 111 128434.857 2.462 0.104 50.18488 1.92 ug/L Cd 114 288038.006 2.065 0.233 49.08887 1.52 ug/L > In 115 1235665.329 0.557 1235665.329 ug/L Sb 121 413423.059 1.406 0.335 49.86756 1.73 ug/L Sb 123 322020.610 2.093 0.261 51.18349 1.53 ug/L Ba 135 155371.067 0.879 0.092 63.49545 2.30 ug/L Ba 137 258697.360 2.329 0.153 62.51790 3.62 ug/L Ho 165 1694099.434 3.778 0.051 ug/L > Tb 159 1690827.941 1.461 1690827.941 ug/L Hg 201 4961.070 2.455 0.003 4.25784 2.98 ug/L Hg 202 11782.750 1.477 0.007 4.39420 2.94 ug/L TI 205 1177412.544 2.349 0.696 50.06985 3.32 ug/L Pb 208 1653941.679 0.589 0.977 49.77206 0.87 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 117.946 > Sc-1 45 72.496 Cr 52 101.593

Sample ID: AE08954 Report Date/Time: Friday, May 03, 2002 14:35:41 Page 1

NYC-WTC_000053045

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