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ICPMS daily performance check report, May 8, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09151 Sample Date/Time: Wednesday, May 08, 2002 11:18:36 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09151.787 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 20528.032 2.465 0.043' 53.92662 2.87 ug/L > Se-1 45 478127.630 3.306 478127.630 ug/L Cr 52 516553.518 4.604 1.064 48.51759 1.32 ug/L Cr 53 62788.800 2.460 0.130 49.24761 1.01 ug/L Wn 55 1373753.150 3.589 2.861 77.91268 3.86 ug/L Ni 60 150111.572 3.896 0.314 53.47571 0.69 ug/L Cu 63 328387.410 2.652 0.686 52.25482 1.49 ug/L Cu 65 164567.184 0.730 0.344 53.33511 2.63 ug/L Zn 66 114074.609 2.175 0.877 52.81872 2.88 ug/L Zn 67 19696.523 2.842 0.151 50.37701 2.60 ug/L Zn 68 85985.098 2.620 0.660 52.36693 0.49 ug/L Ge 72 129281.661 2.153 129281.661 ug/L As 75 146459.904 1.729 1.043 50.36984 1.54 ug/L Se 77 14917.659 1.339 0.104 55.08022 2.05 ug/L Se 82 15810.284 2.851 0.123 54.41268 1.71 ug/L Kr 83 4315.401 0.785 -146.072 ug/L Ag 107 713042.675 0.685 0.384 45.00086 1.66 ug/L in 115 1856500.152 1.693 1856500.152 ug/L Sb 121 644901.610 0.388 0.347 50.77901 2.04 ug/L Sb 123 494845.268 0.402 0.267 50.96567 2.04 ug/L Ba 135 243798.686 1.476 0.090 61.24232 1.44 ug/L Ba 137 425082.659 1.630 0.157 60.97626 1.61 ug/L Tb 159 2712811.036 0.321 2712811.036 ug/L Hg 201 7746.379 3.269 0.003 4.10993 3.34 ug/L Hg 202 17519.716 2.791 0,006 4.11903 2.77 ug/L TI 205 1874629.091 1.622 0.690 45.07212 1.79 ug/L Pb 208 2546766.652 0.871 0.938 46.09925 0.94 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 107.824 > Sc-1 45 93.501 Cr 52 96.802 Cr 53 97.886 Mn 55 102.357

Sample ID: AE09151 Report Date/Time: Wednesday, May 08, 2002 11:21:01 Page 1

NYC-WTC_000053117

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