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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09332 Sample Date/Time: Wednesday, May 08, 2002 12:08:08 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09332.797 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 13,000 27.735 0.000' 0.00571 189.65 ug/L Se-1 45 478548.461 3.706 478548.461 ug/L Cr 52 9729.301 1.097 0.004 0.20145 14.28 ug/L Cr 53 1996.906 3.094 0.003 0.95348 11.07 ug/L Mn 55 530430.628 2.486 1.095 29.82741 2.34 ug/L Ni 60 1389.787 9.112 0.003 0.46145 8.60 ug/L Cu 63 53657.758 0.413 0.112 8.50473 3.77 ug/L Cu 65 26428.297 1.716 0.055 8.51259 3.51 ug/L Zn 66 3921.218 2.272 0.025 1.51934 1.69 ug/L Zn 67 864.383 0.735 0.006 1.84003 1.55 ug/L Zn 68 3627.427 2.413 0.024 1.88997 2.23 ug/L > Ge 72 125966.361 1.090 125966.361 ug/L As 75 12099.012 4.144 0.006 0.29601 48.12 ug/L Se 77 1520.979 3.185 0.000 0.09882 140.59 ug/L Se 82 -54.986 218.679 0.000 0.02206 1922.52 ug/L Kr 83 4214.019 1.256 -247.454 ug/L Ag 107 138.336 7.593 -0.000 -0.01731 3.79 ug/L > In 115 1831194.276 0.845 1831194.276 ug/L Sb 121 629.028 2.786 0.000 0.04062 2.41 ug/L Sb 123 503.651 2.099 0.000 0.04187 2.34 ug/L Ba 135 62973.696 1.713 0.023 15.89040 0.87 ug/L Ba 137 108899.269 1.905 0.040 15.69196 1.16 ug/L > Tb 159 2698781.388 1.227 2698781.388 ug/L Hg 201 90.668 18.986 -0.000 -0.01885 48.21 ug/L Hg 202 206.004 5.045 -0.000 -0.01495 13.90 ug/L n 205 1072.408 10.179 -0.000 -0.01383 17.51 ug/L Pb 208 19490.352 1.864 0.006 0.30118 1.22 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 > Sc-1 45 93.583 Cr 52 Cr 53 Mn 55

Sample ID: AE09332 Report Date/Time: Wednesday, May 08, 2002 12:09:49 Page 1

NYC-WTC_000053137

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