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ICPMS daily performance check report, May 3, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV CALBK Sample Date/Time: Friday, May 03, 2002 13:52:11 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV CAL BK.737 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 8.333 13.856 -0.000' -0.00339 70.13 ug/L > Se-1 45 510746.859 1.563 510746.859 ug/L Cr 52 8540.095 1.110 0.001 0.04733 16.23 ug/L Cr 53 1085.742 3.400 0.001 0.28204 13.47 ug/L Mn 55 950.393 14.279 -0.003 -0.07783 9.21 ug/L Ni 60 216.671 3.925 -0.000 -0.00099 500.88 ug/L Cu 63 394.346 7.039 0.000 0.00098 684.00 ug/L Cu 65 204.671 4.820 0.000 0.00952 29.01 ug/L Zn 66 1178.422 4.929 0.000 0.00656 513.36 ug/L Zn 67 295.008 10.990 0.000 0.13318 75.08 ug/L Zn 68 932.057 0.929 0.000 0.01829 46.00 ug/L > Ge 72 102888.680 0.912 102888.680 ug/L As 75 8068.472 2.659 0.002 0.09339 146.59 ug/L Se 77 1066.206 2.226 0.000 0.12241 146.64 ug/L Se 82 3063.214 2.500 0.001 0.36807 128.13 ug/L Ag 107 153.003 8.497 -0.000 -0.01877 6.86 ug/L Cd 111 45.667 24.121 -0.000 -0.00507 76.91 ug/L Cd 114 106.423 8.084 -0.000 -0.00522 28.25 ug/L > in 115 1338152.671 0.703 1338152.671 ug/L Sb 121 40.000 17.500 0.000 0.00006 1289.45 ug/L Sb 123 43.062 6.694 0.000 0.00051 81.73 ug/L Ba 135 58.667 8.579 0.000 0.00268 73.30 ug/L Ba 137 84.335 11.208 0.000 0.00056 365.68 ug/L Ho 165 1812534.217 2.767 0.033 ug/L > Tb 159 1841197.310 0.385 1841197.310 ug/L Hg 201 58.334 7.730 -0.000 -0.00331 104.01 ug/L Hg 202 135.002 1.960 0.000 0.00936 10.40 ug/L TI 205 422.681 4.031 -0.000 -0.00964 7.44 ug/L Pb 208 1977.437 1.477 -0.000 -0.00137 50.96 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 83.332 Cr 52

Sample ID: CCV CALBK Report Date/Time: Friday, May 03, 2002 13:54:39 Page 1

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NYC-WTC_000053033Source: NYC Law Department, mirrored locally

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