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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV CAL BK Sample Date/Time: Tuesday, May 14, 2002 10:30:41 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV CAL BK.023 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 7.667 7.531 -0.000 - -0.00259 46.91 ug/L > Se-1 45 611811.962 0.722 611811.962 ug/L Cr 52 9009.887 1.644 -0.000 -0.01568 47.20 ug/L Cr 53 1163.753 1.754 0.000 0.18056 10.11 ug/L Mn 55 1088.743 5.965 -0.000 -C .00496 56.18 ug/L Ni 60 48.667 12.555 0.000 0.00314 60.88 ug/L Cu 63 329.676 9.690 -0.000 -0.00085 585.22 ug/L Cu 65 194.004 9.449 0.000 0 00762 67.99 ug/L Zn 66 909.721 5.659 -0.001 -0.05017 33.59 ug/L Zn 67 202.338 2.979 0.000 0 02546 58.87 ug/L Zn 68 639.029 0.542 -0.001 -0 08575 8.90 ug/L > Ge 72 128606.445 1.888 128606.445 ug/L As 75 5843.250 1.339 0.001 0.04211 150.71 ug/L Se 77 847.578 1.532 0.000 0.02656 88.37 ug/L Se 82 -74.972 37.988 -0.000 -0.20834 47.00 ug/L Kr 83 2333.323 0.827 -171.381 ug/L Ag 107 260.340 16.842 -0.000 -0.0)511 62.67 ug/L In 115 1685352.218 1.002 1685352.218 ug/L Sb 121 66.001 16.035 0.000 0.0 1327 31.04 ug/L Sb 123 49.856 25.084 0.000 0.0 1240 63.67 ug/L Ba 135 64.668 18.706 0.000 0.0 1284 129.14 ug/L Ba 137 86.668 18.653 -0.000 -0.00136 205.44 ug/L Tb 159 2699403.493 1.079 2699403.493 ug/L Hg 201 38.000 5.263 -0.000 -0.00507 28.11 ug/L Hg 202 80.334 13.712 -0.000 -0.0(417 74.02 ug/L TI 205 1083.743 13.554 0.000 0.00304 127.92 ug/L Pb 208 2826.866 0.805 -0.000 -0.00246 6.24 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff ' Be 9 > Sc-1 45 86.819 Cr 52 Cr 53 Mn 55

Sample ID: CCV CAL BK Report Date/Time: Tuesday, May 14, 2002 10:32:59 Page 1

NYC-WTC_000053434

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