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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV CAL BK Sample Date/Time: Tuesday, May 14, 2002 12:01:38 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV CAL BK.039 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.333 49.661 0.000 0.00296 357.34 ug/L Se-1 45 606516.813 1.268 606516.813 ug/L Cr 52 8834.714 2.518 -0.000 -0.02317 59.25 ug/L Cr 53 909.722 9.473 0.000 0.02247 282.89 ug/L Mn 55 912.055 1.236 -0.000 -0.01263 8.24 ug/L Ni 60 54.334 8.299 0.000 0.00504 28.89 ug/L Cu 63 350.677 6.052 0.000 0.00261 120.10 ug/L Cu 65 188.671 7.427 0.000 0.00650 56.77 ug/L Zn 66 860.716 3.256 -0.001 -0.06610 25.10 ug/L Zn 67 181.670 9.990 -0.000 -0.02088 236.61 ug/L Zn 68 668.365 4.063 -0.001 -0.06120 32.13 ug/L Ge 72 126594.311 0.888 126594.311 ug/L As 75 5974.734 1.329 0.003 0.12747 36.11 ug/L Se 77 850.062 0.842 0.000 0.09193 50.04 ug/L Se 82 -59.191 143.480 -0.000 -0.15558 189.89 ug/L Kr 83 2358.996 2.232 -145.707 ug/L Ag 107 267.007 4.221 -0.000 -0.0)483 17.36 ug/L > In 115 1700190.783 0.381 1700190.783 ug/L Sb 121 43.334 10.906 0.000 0.00106 41.92 ug/L Sb 123 37.983 38.805 0.000 0.00087 212.68 ug/L Ba 135 65.334 3.852 0.000 0.00285 30.48 ug/L Ba 137 99.002 9.636 0.000 0.00052 341.63 ug/L Tb 159 2723434.406 1.965 2723434.406 ug/L Hg 201 47.001 13.952 -0.000 -0.00001 42743.10 ug/L Hg 202 100.335 6.485 0.000 0.0C078 152.83 ug/L TI 205 1071.075 15.077 0.000 0.00253 177.43 ug/L Pb 208 2824.199 2.308 -0.000 -0.00300 38.49 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 86.067 Cr 52 Cr 53 Mn 55

Sample ID: CCV CAL BK Report Date/Time: Tuesday, May 14, 2002 12:03:40 Page 1

NYC-WTC_000053466

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