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ICPMS daily performance check report, April 25, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on April 25, 2002.

NYC-WTC_000053337–000053387

Folder label: “ICPMS 4/25/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV CALBK Sample Date/Time: Thursday, April 25, 2002 15:30:37 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\dataset\new york city\CCV CAL BK.711 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Gone. Mean Cone. RSD Sample Unit Be 9 4.000 66.144 -0.000 -0.01538 48.37 ug/L > Se-1 45 482232.696 0.899 482232.696 ug/L Cr 52 6812.287 2.168 -0.001 -0.06725 34.00 ug/L Cr 53 819.045 4.200 0.001 0.25241 12.98 ug/L Mn 55 1297.772 3.277 -0.001 -0.02791 13.91 ug/L Ni 60 148.336 6.651 -0.000 -0.00854 45.52 ug/L Cu 63 339.010 6.024 -0.000 -0.00274 138.12 ug/L Cu 65 202.338 12.758 0.000 0.00350 284.86 ug/L Zn 66 931.390 4.902 -0.000 -0.01932 115.55 ug/L Zn 67 204.004 5.302 0.000 0.09401 50.25 ug/L Zn 68 672.698 7.968 -0.001 -0.07366 60.46 ug/L Ge 72 92662.177 1.514 92662.177 ug/L As 75 63.943 57.148 -0.001 -0.03772 50.20 ug/L Se 77 119.912 6.001 0.000 0.07703 42.12 ug/L Se 82 102.668 9.258 -0.000 -0.05845 67.31 ug/L Ag 107 147.669 9.219 0.000 0.00356 40.93 ug/L > in 115 1250287.671 1.007 1250287.671 ug/L Sb 121 69.001 5.797 0.000 0.00526 7.79 ug/L Sb 123 58.147 12.222 0.000 0.00536 20.08 ug/L Ba 135 37.000 9.745 -0.000 -0.00077 182.83 ug/L Ba 137 59.334 25.244 0.000 0.00206 161.31 ug/L- Ho 165 1693908.098 1.169 -0.002 ug/L > Tb 159 1716396.348 0.289 1716396.348 ug/L Hg 201 47.667 12.646 0.000 0.00325 169.96 ug/L Hg 202 81.335 9.310 0.000 0.00264 117.82 ug/L TI 205 906.721 5.381 -0.000 -0.00571 39.36 ug/L Pb 208 1747.417 5.023 -0.000 -0.00357 84.33 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery l nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 114.997 Cr 52 Cr 53 Mn 55

Sample ID: CCV CALBK Report Date/Time: Thursday, April 25, 2002 15:33:03 Page 1

NYC-WTC_000053382

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