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ICPMS daily performance check report, May 3, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV CALBK Sample Date/Time: Friday, May 03, 2002 16:45:16 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV CAL BK.753 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 8.667 13.323 -0.000 -0.00086 320.26 ug/L Se-1 45 463126.238 5.536 463126.238 ug/L Cr 52 6457.692 2.596 -0.002 -0.08638 64.01 ug/L Cr 53 693.700 6.308 0.000 0.02042 43.90 ug/L Mn 55 430.681 2.094 -0.004 -0.10554 1.75 ug/L Ni 60 192.671 2.663 -0.000 -0.00267 137.06 ug/L Cu 63 500.019 1.562 0.000 0.03221 19.46 ug/L Cu 65 264.006 3.409 0.000 0.04355 12.39 ug/L Zn 66 1678.839 3.933 0.006 0.37747 8.75 ug/L Zn 67 293.008 2.730 0.001 0.20917 17.07 ug/L Zn 68 1235.430 4.454 0.004 0.33450 11.42 ug/L > Ge 72 94581.089 0.790 94581.089 ug/L As 75 7573.840 2.204 0.004 0.17467 46.38 ug/L Se 77 997.832 3.078 0.000 0.22469 70.84 ug/L Se 82 2854.143 1.841 0.001 0.55424 41.94 ug/L Ag 107 120.335 11.674 -0.000 -0.02103 6.01 ug/L Cd 111 55.667 33.624 0.000 0.00008 8754.93 ug/L Cd 114 126.331 34.586 -0.000 / -0.00057 1321.42 ug/L > In 115 1245599.309 1.371 1245599.309 ug/L Sb 121 32.334 15.256 -0.000 -0.00052 120.46 ug/L Sb 123 23.141 9.415 -0.000 -0.00216 15.88 ug/L Ba 135 57.001 6.326 0.000 0.00375 33.22 ug/L Ba 137 82.668 0.698 0.000 0.00165 5.95 ug/L Ho 165 1832700.645 2.026 0.123 ug/L > Tb 159 1705732.131 0.983 1705732.131 ug/L Hg 201 48.667 4.277 -0.000 -0.00794 17.63 ug/L Hg 202 112.668 11.309 0.000 0.00475 101.46 ug/L 71 205 372.678 3.808 -0.000 -0.01044 4.94 ug/L Pb 208 1363.386 4.511 -0.000 -0.01537 9.94 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 75.563 Cr 52

Sample ID: CCV CALBK Report Date/Time: Friday, May 03, 2002 16:47:48 Page 1

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