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ICPMS daily performance check report, May 3, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH . Method 200.8 - Summary Report Sample ID: AE08755 Sample Date/Time: Friday, May 03, 2002 12:00:51 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE08755.726 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 25901.118 2.798 0.050 ' 51.58401 3.33 ug/L > Se-1 45 522156.376 6.124 522156.376 ug/L Cr 52 516569.535 0.256 0.975 47.64878 5.96 ug/L Cr 53 62629.707 2.849 0.119 49.33885 3.32 ug/L Mn 55 998425.951 0.065 1.911 57.15752 6.20 ug/L Ni 60 128044.230 0.697 0.245 52.28201 6.83 ug/L Cu 63 262247.693 1.347 0.502 50.74117 4.79 ug/L Cu 65 132222.946 0.577 0.253 50.64800 6.71 ug/L Zn 66 93401.986 2.855 0.881 51.93228 1.04 ug/L Zn 67 15837.943 0.698 0.149 48.78032 2.57 ug/L Zn 68 71796.110 0.387 0.677 53.54690 2.24 ug/L > Ge 72 104640.422 1.826 104640.422 ug/L As 75 121649.880 1.091 1.086 53.76724 0.79 ug/L Se 77 11746.175 3.110 0.102 56.50563 1.41 ug/L Se 82 15451.277 2.155 0.119 55.44550 0.41 ug/L Ag 107 476735.514 0.243 0.368 46.53277 0.94 ug/L Cd 111 139036.150 1.590 0.107 51.89207 0.41 ug/L Cd 114 308109.803 1.441 0.238 50.16394 2.63 ug/L In 115 1293728.243 1.183 1293728.243 ug/L Sb 121 436833.458 1.529 0.338 50.32335 0.35 ug/L Sb 123 350399.398 0.359 0.271 53.20043 0.82 ug/L Ba 135 163544.137 0.937 0.091 63.11143 2.00 ug/L Ba 137 290658.472 1.770 0.162 66.31258 0.71 ug/L Ho 165 1860969.106 1.191 0.088 ug/L > Tb 159 1790390.148 1.060 1790390.148 ug/L Hg 201 6145.639 3.627 0.003 4.98818 2.59 ug/L Hg 202 14188.708 2.081 0.008 5.00063 1.03 ug/L TI 205 1275305.723 2.491 0.712 51.20076 1.43 ug/L Pb 208 1696079.200 0.771 0.946 48.19669 0.29 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff " Diff Be 9 103.166 Se-1 45 85.194 Cr 52 94.745

Sample ID: AE08755 Report Date/Time: Friday, May 03, 2002 12:02:51 Page 1

NYC-WTC_000053000

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