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ICPMS daily performance check report, April 25, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on April 25, 2002.

NYC-WTC_000053337–000053387

Folder label: “ICPMS 4/25/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08960 Sample Date/Time: Thursday, April 25, 2002 14:57:55 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\dataset\new york city\AE08960.701 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 18405.130 0.681 0.041 54.07433 2.44 ug/L Sc-1 45 453470.868 2.397 453470.868 ug/L Cr 52 413461.617 0.188 0.897 48.62123 2.48 ug/L Cr 53 48842.009 0.426 0.107 48.65215 2.22 ug/L Mn 55 850355.477 0.315 1.872 65.03823 2.28 ug/L Ni 60 99162.251 1.084 0.218 47.72098 1.37 ug/L Cu 63 268968.156 2.507 0.592 57.05571 0.79 ug/L Cu 65 132274.815 1.484 0.291 56.69920 1.18 ug/L Zn 66 80480.491 0.890 0.888 52.78539 0.50 ug/L Zn 67 14391.526 0.555 0.159 51.64889 0.92 ug/L Zn 68 60888.505 0.572 0.671 53.23966 1.17 ug/L > Ge 72 89629.612 1.275 89629.612 ug/L As 75 91185.244 1.398 1.016 50.50287 2.10 ug/L Se 77 8951.042 1.467 0.099 54.79964 1.92 ug/L Se 82 10791.177 1.909 0.119 53.72366 1.89 ug/L Ag 107 450493.997 1.906 0.374 46.15237 2.26 ug/L In 115 1204023.030 0.454 1204023.030 ug/L Sb 121 414743.469 0.350 0.344 51.10790 0.62 ug/L Sb 123 319159.431 0.387 0.265 50.66785 0.31 ug/L Ba 135 159934.621 1.146 0.098 65.41561 0.36 ug/L Ba 137 277014.343 1.251 0.171 64.89220 0.85 ug/L Ho 165 1613344.548 0.365 0.005 ug/L Tb 159 1624372.302 0.882 1624372.302 ug/L Hg 201 4287.387 1.769 0.003 4.17877 1.69 ug/L Hg 202 9691.594 0.800 0.006 4.16202 0.22 ug/L TI 205 1049521.779 1.662 0.645 48.71996 1.14 ug/L Pb 208 1429130.077 1.301 0.879 49.22312 0.42 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 108.159 > Sc-1 45 108.138 Cr 52 96.926 Cr 53 96.617 Mn 55 97.715

Sample ID: AE08960 Report Date/Time: Thursday, April 25, 2002 15:00:28 Page 1

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