GCMS analysis report for sample AE01226, Feb 2002

NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\FEB1502\1226.D Vial: 26 Acq On : 16 Feb 2002 5:38 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3,4-Dimethyl-5-hexen-3-ol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.42 ug/1 37475 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual _ ____________ 1 3,4-Dimethyl/5-hexen-3-ol 128 C8H160 000000-00-0 9 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3 -Dioxolane 74 C3H602 000646-06-0 5 Abundance Scan 346 (8.216 min): 1226.D (-) m/z73.00100.00% 73

5000 43

7.80 8.00 8.20 8.40 8.60 . 1| | , . 55... , I , , 1 ■ i 11 ■ 1 I 111 । l^"1 1 ' 1 1 84............. 199. , m/z 43.05 40.84% m/z-> 10 20 30 40 50 60 70 80 90 100 110 : Abundel ce #5018: 3.4-Dimethyl-5-hexen-3-oi 73

43 5000 55 / Umm 7.80 8.00 8.20 8.40 8.60 27 m/ z ( 16.29% 67! ' ' I 81. । । , 99 । । , , miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance c an 73 —— 7.80 8.00 8.20 8.40 8.60 5000- 45 m/ z 44.95 14.41%

27 33 39 55 ■ ■ । ' 1 1 ■ । ' ' i ' ' ' ' i ■ 1 ' ' i ' ' ' ■ i 1 1 ■ ■ i ■ ' ' ' i ' ' ■ ' i ■ ■ ■ ■ i ■ 1 1 1 i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abdr j nice #845: Silane, tetramethyl- 73 7.80 8.00 8.20 8.40 8.60 m/ z 39.05 7.78% 5000

m/z- i ' ' 10 15 ■ ' 31 i ' ' ’ ' i' ■ 20 30 45 | 55 ' i 1 11 ■ I 1 1'' i11 । 40 50 60 70 1............. 88............................. 80 90 100 110 h...... 14...., 7.80 8.00 8.20 8.40 8.60

1226.D GCMS0208.M Wed Feb 20 14:31:36 2002 Page 1

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