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GCMS analysis report for sample AE01226, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01226 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052805–000052814

Folder label: “GCMS X 1/17/02 A 2/16/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\1226.D Vial: 26 Acq On : 16 Feb 2002 5:38 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethylene oxide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

18.10 0.26 ug/1 28658 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual _________________ [_______________________________________ 1 Ethylene' oxide 44 C2H40 000075-21-8 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Propane 44 C3H8 000074-98-6 1 4 Carbamic acid, monoammonium salt 78 CH6N202 001111-78-0 1 Abundance ( Scan 1423 (18.104 min): 1226.D (-) m/ z 39.95 100.00% 40 44 5000

17.80 18.00 18.20 18.40 36 38 49 m/ Z . < r< 11 ।. 11. <.. (. <.. ।.... । <. > > ।. r«.. r... ।. r । ।. > < > ।. r... ।. <. < । ।।. 43.95 49.63% m/z-> 2 4 6 8 10 12 14 1618 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 Abu iro #37: Ethylene oxide 29

15 44 5000 Tr 17.80 18.00 18.20 18.40 42 m/ z 36.00 1.43% 13 : 24,26. mpmpmpmmmmgmmmpmp 31 TT m/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 Abundance ■ . . 29 44

17.80 18.00 18.20 18.40 5000 m/ z 44.95 0.86%

42 >i 1111■ 111■ >।। ।t 24 26 31 40 TTCITTTTUT"TTT‘T ।।■ it i| ■ ■ iil<■ ।■ ■ ■ ■ ।>iM,.Mipi

m/z-> 2 4 6 8 1012 14 1618 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 Abundance #62269: Propane ■ i ' ■ ' ■ i ' ■ 29 17.80 18.00 18.20 18.40 m/ z 37.90 0.68% 5000 27 44 15 3941 ...... T" — .... . mnnd"mH"IENT TEITTITI’TT m/z-> 2 4 6 8 1012 14 1618 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 17.80 18.00 18.20 18.40

1226.D GCMS0208.M Wed Feb 20 14:31:41 2002 Page 2

NYC-WTC_000052813

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NYC-WTC_000052813Source: NYC Law Department, mirrored locally

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