GCMS calibration results for sample AE01041, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

4 Data File : C:\HPCHEM\l\DATA\FEB1502\CAL10A.D Vial: 2 Acq On : 16 Feb 2002 2:43 pm Operator: 209 GALOS Sample : gc/ms scan 2/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 13:56 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.34 152 455716 20.00 ug/1 -0.01 10) Naphthalene-d8 15.98 136 1783143 20.00 ug/1 -0.01 17) Acenaphthene -dl0 21.30 164 980074 20.00 ug/1 -0.01 29) Phenanthrene-dlO 25.74 188 1445201 20.00 ug/1 -0.02 38) Chrysene-dl2 33.81 240 1023560 20.00 ug/1 -0.03 44) Perylene-dl2 38.10 264 656798 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.96 74 183921 10.09 ug/1 99 3) bis(2-Chloroethyl)ether 11.74 93 306364 10.23 ug/1 99 4) 1,3-Dichlorobenzene 12.24 146 345901 9.70 ug/1 98 5) 1,4-Dichlorobenzene 12.39 146 355388 9.78 ug/1 99 6) 1,2-Dichlorobenzene 12.90 146 344811 9.99 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.21 45 474394 10.46 ug/1 98 8) N-Nitroso-di-n-propylamine 13.62 70 222758 10.40 ug/1 97 9) Hexachloroethane 13.74 117 141381 9.72 ug/1 95 11) Nitrobenzene 14.03 77 359761 9.81 ug/1 100 12) Isophorone 14.67 82 604283 9.76 ug/1 100 13) bis(2-Chloroethoxy)methane 15.35 93 368328 9.55 ug/1 98 14) 1,2,4-Trichlorobenzene 15.87 180 287091 9.41 ug/1 96 15) Naphthalene 16.04 128 904731 9.53 ug/1 100 16) Hexachlorobutadiene 16.58 225 175830 9.63 ug/1 98 18) 19) Hexachlorocyclopentadiene 2-Chloronaphthalene 18.78 19.55 237 162 107316 545687 (7.65 ug/1 98 9.34 ug/1 99 20) Dimethylphthalate 20.64 163 653100 9.60 ug/1 100 21) 2,6-Dinitrotoluene 20.85 165 147244 9.55 ug/1 98 22) Acenaphthylene 20.82 152 815295 9.66 ug/1 100 23) Acenaphthene 21.39 153 573402 9.72 ug/1 99 24) 2,4-Dinitrotoluene 22.03 165 186151 9.53 ug/1 98 25) Diethylphthalate 22.78 149 692691 9.79 ug/1 99 26) 4-Chlorophenyl-phenylether 22.92 204 303220 9.96 ug/1 100 27) Fluorene 22.91 166 632122 9.82 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.39 77 708052 9.52 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0208.M Wed Feb 20 13:57:04 2002 Page 1

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